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1.This article discusses the acidic potassium permanganate method of permanganate index from the following aspects: heating time, titrate temperature and titrate speed, end point of titration.
摘要文章对高锰酸盐指数加热时间、滴定温度、速度、滴定的控制进行了探讨。收藏指正
2.1mol/LKCI solution as ionic strength adjustor(ISA),the titrant is fed in a step way in equivalent Volumes to determine the pH value. After titration of weak base with strong acid,the volume of the titrant Vt is graphed in terms of Gran func- tion(V_0+V_t)×10~(-pH). The end point of titration can be derived by method of straight line extrapolation.
该法以0.1 mol/l KCl溶液为离子强度调节剂(ISA),分步等体积滴入滴定剂,测定相应的pH值,按强酸滴定弱碱计量后之Gran函数(V_0+V_t)×10~(-pH)州对滴定剂体积V_t作图,用直线外推法求滴定收藏指正
3.Pefloxacin mesylate was precipitated as PEFM TPB in HCl NaAc buffer solution (pH=5.2). After filtering off the precipitate, the excessive sodium tetraphenylboron in the filtrate was titrated with thallous sulfate standard solution in an alkaline solution. The disappearance of the incision of TPB on dE/dt=f (E) curve was used to indicate the end point of titration.
在 pH5 2的HCl NaAc缓冲溶液中 ,四苯硼钠 (Na TPB)与甲磺酸培氟沙星作用可生成 1∶1定量沉淀 ,过滤弃去初滤液 ,用硫酸亚铊标准溶液滴定续滤液中过量的Na TPB ,通过示波极谱图 (dE/dt=f(E)曲线 )上TPB的切口消失指示滴定收藏指正
4.The result shows that the titration end point of cobalt with EDTA standard soultion as titrant was found to be sharp in the buffer solution of NH 3 · H 2 O-NH 4 Ac (pH=7.0) containing five drops TTZDBA solution. The end point occurs when the solution colour changes from purple red to bright orange, the end point is sensitive.
在pH值为 7.0的NH3 ·H2 O -NH4Ac缓冲溶液中 ,加入 5滴TTZDBA作指示剂 ,用EDTA标准溶液进行滴定 ,滴定溶液的颜色变化敏锐 ,由紫红色变为亮橙色。收藏指正
5.The results indicated that the end-point for the titration of cobalt with eight drops of the reagent solution was found to be sharper in NH_3·H_2O-NH_4Ac buffer solution at pH 4.0-7.0,and the color of solution at terminal point turned from mauve into bright orange.
结果表明,在pH 4.0~7.0的NH3.H2O-NH4Ac缓冲溶液中,加入8滴1.0 g/L指示剂CTZDBA溶液,用EDTA标准溶液进行滴定,滴定由紫红色变为亮橙色,变色敏锐,准确度高。收藏指正
6.A simple method for alternate current oseillopolarographic titration of aluminium and titanium with zinc acetate is described. In a buffer solution of pH=6(HAc-NH_4Ac)a sharp Zn~(2+) incision appears on dE/dt=f(E) curves, which can be used to indicate the end point.
本文在pH6的HAc-NH_4Ac缓冲溶液中,用乙酸锌标准溶液滴定铝和钛,以Zn~(2+)在交流示波极谱dE/dt=f(E)曲线上出现切口直接指示。 方法准确、可靠,并用于硅酸盐岩石中铝和钛的测定,结果令人满意。收藏指正
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