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1.The non isothermal decomposition process and decomposition kinetics of analginum in static atmosphere were studied by TG DTG techniques. The middle and finial product were determined by TG DTG curves and IR diagrams. The data were analysized by differential and integral methods.
采用 TG- DTG技术研究了安乃近在静态空气气氛中的非等温热分解过程及其动力学 ,根据 TG曲线并结合红外光谱技术确定了热分解过程中的中间产物及最终产物 ,运用微分法和积分法对热分析数据进行了分析 ,推断出第 1步反应为脱水反应 ,其动力学方程为 dα/ dt=Ae-ERT(1-α) ;收藏指正
2.The oxidation of CaS was studied in the temperature range of 970~1150℃ under O2 atmosphere with different O2 concentrations. Experiments were carried out by a Metteler Toledo TGA instrument under isothermal condition and the exhausted gas was analyzed by the infrared spectral method.
采用热重等温实验研究了970~1150℃内CaS的氧化反应特性,利用红外光谱仪定量分析反应析出SO2气体,通过亚甲基蓝分光光度法测定固体残留物中CaS的含量。收藏指正
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