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1.Amount of acetic anhydride is main factor,temperature of reaction,amount of activation catalyst are secondary factors and the best reaction condition are as follows:activated starch is 15.87 g,reaction temperature is 70℃,acetic anhydride is 28 g,oil of vitriol is 0.7 g. Under these conditions we will obtain high substitute starch acetate(DS=2.465).
最佳反应条件:活化淀粉15.87 g,反应温度70℃,醋酸酐用量28 g,催化剂浓硫酸用量0.7 g,在此条件下制得的淀粉醋酸酯的取代度DS=2.465。收藏指正
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