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1.The equilibrium adsorbate uptake we is 5.6 times that of macro-porous silica gel, 3.4 times that of micro-porous silica gel and 1.17 times that of synthetic zeolite 13X.
实验表明,这种复合吸附剂的平衡吸附量we最大可达0.263kg H2O/kg干吸附剂,是粗孔球形硅胶的5.6倍、细孔球形硅胶的3.4倍、分子筛13X的1.17倍。收藏指正
2.Highly siliceous faujasite was prepared by dealumination of synthetic Y-type zeolite and was then modified with (NH_4)_2SiF_6. The decay of cracking activity and coke deposition on SiCl_4 modified zeolites,Y(T-1,2,3),were compared with those modified with SiF_6, FSY-l,2,3,by catalytic cracking of cumene in a continuous laboratory reactor.
HY经脱铝制得高硅八面沸石,并经SiCl_4和(NH_4)_2SiF_6分别改性后的样品称之为Y(T)和FSY. 采用异丙苯裂化反应比较了它们的活性衰减与结焦之间的关系.收藏指正
3.A new type of mesoporous aluminosilicate, named SAN-01, was synthesized with microcline as raw materials by integrating the synthetic procedures of MCM-41 and 13X zeolite.
本研究以天然微斜长石为原料,结合介孔分子筛MCM-41与13X沸石合成工艺,合成了孔壁中含有13X沸石基本结构单元D6R的铝硅酸盐介孔分子筛, 命名为SAN-01。收藏指正
4.MCM-22 zeolite was synthesized with an organic mixture solution (OMS) yielded from the hydrogenation of caprolactam as a template. The effects of crystallization conditions on the synthetic products were investigated.
以己内酰胺催化加氢得到的有机混合物水溶液 (OMS)为模板剂合成了纯MCM 2 2分子筛 ,考察了晶化条件对合成产物的影响。收藏指正
5.The optimum synthetic conditions of ethyl chloroacetate are: molar ratio of chloroacetic acid to ethanol is 1:8, the quantity of catalyst[Fe2(SO4)3 xH2O] is 10% of the mass of chloroacetic acid, reaction time is 1 hour, 5A zeolite was used as dehydrating agent. In these conditions, the yield of ethyl chloroacetate was up to 73%.
用Fe_2(SO_4)_3·xH_2O作为催化剂合成氯乙酸乙酯的较佳反应条件是:酸醇物质的量之比为1:8,催化剂用量为氯乙酸质量的10%,以5A分子筛作为脱水剂,回流时间1h,收率达73%以上。收藏指正
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